Synthesis of 2,6-bis(1,i>H -imidazole-2-yl)-4-chloropyridine

I. A. Os’kina; Оськина И. А.; L. G. Lavrenova; Лавренова Л. Г.; A. Ya. Tikhonov; Тихонов А. Я.

doi:10.31857/S0514749225030164

Synthesis of 2,6-bis(1,i>H-imidazole-2-yl)-4-chloropyridine

作者: Os’kina I.A.¹, Lavrenova L.G.², Tikhonov A.Y.¹
隶属关系:
1. Vorozhtsov Novosibirsk Institute of Organic Chemistry, Siberian Branch, Russian Academy of Sciences
2. Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences
期: 卷 61, 编号 3 (2025)
页面: 338-340
栏目: КРАТКОЕ СООБЩЕНИЕ
URL: https://manmiljournal.ru/0514-7492/article/view/687766
DOI: https://doi.org/10.31857/S0514749225030164
EDN: https://elibrary.ru/EVDLPM
ID: 687766

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详细

On the basis of helidamic acid, 4-chloropyridine-2,6-dicarboxamide and 4-chloropyridine-2,6-dicarbonitrile were synthesized sequentially, the interaction of which with diethyl acetal aminoacetaldehyde led to 2,6-bis(1H-imidazole-2-yl)-4-chloropyridine, a tridentate ligand.

关键词

helidamic acid, 4-chloropyridine-2, 6-dicarboxamide, 4-chloropyridine-2, 6-dicarbonitrile, 2, 6-bis(1H-imidazole-2-yl)-4-chloropyridine

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作者简介

I. Os’kina

Vorozhtsov Novosibirsk Institute of Organic Chemistry, Siberian Branch, Russian Academy of Sciences

编辑信件的主要联系方式.
Email: oi@nioch.nsc.ru
ORCID iD: 0000-0001-5788-0182
俄罗斯联邦, prosp. Akad. Lavrentieva, 9, Novosibirsk, 630090

L. Lavrenova

Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences

Email: oi@nioch.nsc.ru
ORCID iD: 0000-0003-4451-1630
俄罗斯联邦, pr. Akademika Lavrent’eva, 3, Novosibirsk, 630090

A. Tikhonov

Vorozhtsov Novosibirsk Institute of Organic Chemistry, Siberian Branch, Russian Academy of Sciences

Email: oi@nioch.nsc.ru
ORCID iD: 0000-0002-6391-4366
俄罗斯联邦, prosp. Akad. Lavrentieva, 9, Novosibirsk, 630090

参考

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Shakirova O.G., Os'kina I.A., Korotaev E.V., Petrov S.A., Kuratieva N.V., Tikhonov A.Ya., Lavrenova L.G. Int. J. Mol. Sci. 2023, 24, 9853. doi: 10.3390/ijms24129853
La Tour J.V., Wallis K.P., Le P., Hoss U. Пат. US20220202326A1 (2022). США. C.A. 2023, 179, 170111.
Hommes P., Fischer C., Lindner C., Zipse H., Reissig H.-U. Angew. Chem. Int. Ed. 2014, 53, 7647–7651. doi: 10.1002/anie.201403403
Wu K.-L., Ho S.-T., Chou C.-C., Chang Y.-C., Pan H.-A., Chi Y., Chou P.-T. Angew. Chem. Int. Ed. 2012, 51, 5642–5646. doi: 10.1002/anie.201200071